Regl. 6302, art. 405(b)(9)-4 dup2
2, or if the difference between the two average
Length: 2,108 wordsOfficial source
Cite as Reglamento Núm. 6302, Art. 405(b)(9)-4 dup2
opacity values is less than 2 percent opacity. To conduct
this demonstration, measure the opacities at the two locations or paths for a minimum period of 2 hours and compare the results. The opacities of the two locations or
paths may be measured at different times, but must be
measured at the same process operating conditions. Alternative procedures for determining acceptable locations
may be used if approved by the Administrator.
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Pt. 60, App. B, Spec. 1
5. Design and Performance Specifications
5.1 Design Specifications. The CEMS for opacity
shall comply with the following design specifications:
5.1.1 Peak and Mean Spectral Responses. The peak
and mean spectral responses must occur between 500 nm
and 600 nm. The response at any wavelength below 400
nm or above 700 nm shall be less than 10 percent of the
peak spectral response.
5.1.2 Angle of View. The total angle of view shall be
no greater than 5 degrees.
5.1.3 Angle of Projection. The total angle of projection shall be no greater than 5 degrees.
5.1.4 Optical Alignment Sight. Each analyzer must
provide some method for visually determining that the instrument is optically aligned. The method provided must
be capable of indicating that the unit is misaligned when
an error of +2 percent opacity occurs due to misalignment
at a monitor path length of 8 meters. Instruments that are
capable of providing an absolute zero check while in operation on a stack or duct with effluent present, and while
maintaining the same optical alignment during measurement and calibration, need not meet this requirement
(e.g., some "zero pipe" units).
5.1.5 Simulated Zero and Upscale Calibration System.
Each analyzer must include a calibration system for simulating a zero (or no greater than 10 percent) opacity and
an upscale opacity value for the purpose of performing
periodic checks of the transmissometer calibration while
on an operating stack or duct. This calibration system will
provide, as a minimum, a system check of the analyzer
internal optics and all electronic circuitry including the
lamp and photodetector assembly.
5.1.6 Access to External Optics. Each analyzer must
provide a means of access to the optical surfaces exposed
to the effluent stream in order to permit the surfaces to
be cleaned without requiring removal of the unit from the
source mounting or without requiring optical realignment
of the unit.
5.1.7 Automatic Zero Compensation Indicator. If the
CEMS has a feature that provides automatic zero compensation for dirt accumulation on exposed optical surfaces, the system must also provide some means of indicating when a compensation of 4 percent opacity has been
exceeded. This indicator shall be at a location accessible
to the operator (e.g., the data output terminal). During the
operational test period, the system must provide some
means (manual or automated) for determining the actual
amount of zero compensation at the specified 24-hour intervals so that the actual 24-hour zero drift can be determined (see Section 7.4.1).
5.1.8 Slotted Tube. For transmissometers that use
slotted tubes, the length of the slotted portion(s) must be
equal to or greater than 90 percent of the effluent path
length (distance between duct or stack walls). The slotted
tube must be of sufficient size and orientation so as not
to interfere with the free flow of effluent through the cntire optical volume of the transmissometer photodetector.
The manufacturer must also show that the transmissometer minimizes light reflections. As a minimum, this
demonstration shall consist of laboratory operation of the
transmissometer both with and without the slotted tube in
position.
Should the operator desire to use a slotted tube design
with a slotted portion equal to or less than 90 percent of
the monitor path length, the operator must demonstrate to
the Administrator that acceptable results can be obtained.
As a minimum demonstration, the effluent opacity shall
be measured using both the slotted tube instrument and
another instrument meeting the requirement of this specification but not of the slotted tube design. The measurements must be made at the same location and at the same
process operating conditions for a minimum period of 2
hours with each instrument. The shorter slotted tube may
be used if the average opacity measured is equivalent to
the opacity measured by the nonslotted tube design. The
average opacity measured is equivalent if it is within the
opacity range defined by the average opacity value +10
percent measured by the nonslotted tube design, or if the
difference between the average opacities is less than 2
percent opacity.
5.1.9 External Calibration Filter Access (optional).
Provisions in the design of the transmissometer to accommodate an external calibration filter assembly are recommended An adequate design would permit occasional
use of external (i.e., not intrinsic to the instrument) neutral density filters to assess monitor operation.
5.2 Performance Specifications. The opacity CEMS
specifications are listed in Table 1-1.
6. Design Specifications Verification Procedure
These procedures will not apply to all instrument designs and will require modification in some cases; all procedural modifications are subject to the approval of the
Administrator.
Test each analyzer for conformance with the design
specifications of Sections 5.1.1-5.1.4, or obtain a certificate of conformance from the analyzer manufacturer as
follows:
6.1 Spectral Response. Obtain detector response, lamp
emissivity, and filter transmittance data for the components used in the measurement system from their respective manufacturers. and develop the effective spectral response curve of the transmissometer. Then determine and
report the peak spectral response wavelength, the mean
spectral response wavelength, and the maximum response
at any wavelength below 400 mm and above 700 nm expressed as a percentage of the peak response.
Alternatively, conduct a laboratory measurement of the
instrument's spectral response curve. The procedures of
this laboratory evaluation are subject to approval of the
Administrator.
TABLE 1-1-PERFORMANCE SPECIFICATIONS
Expressed as the sum of the absolute value of the mean
and the absolute value of the confidence coefficient.
During the conditioning and operational test periods, the
CEMS must not require any corrective maintenance, repair,
replacement, or adjustment other than that clearly specified as
routine and required in the operation and maintenance manuals.
6.2 Angle of View. Set up the receiver as specified
by the manufacturer's written instructions. Draw an are
with radius of 3 meters in the horizontal direction. Using
a small (less than 3 centimeters) nondirectional light
source. measure the receiver response at 5-centimeter intervals on the are for 30 centimeters on either side of the
Parameter
Specifications
1. Calibration BITOR
<3 percent opacity.
2. Response time
s10 seconds.
3. Conditioning period
≤168 hours.
4. Operational test period
$168 hours.
5. Zero drift (24-hour)*
52 percent opacity.
6. Calibration drift (24-hour)
<2 percent opacity.
7. Data recorder resolution
<0.5 percent opacity.
Pt. 60, App. B, Spec. 1
detector centerline. Repeat the test in the vertical direction. Then for both the horizontal and vertical directions,
calculate the response of the receiver as a function of
viewing angle (26 centimeters of are with a radius of 3
meters equals 5 degrees). report relative angle of view
curves, and determine and report the angle of view.
6.3 Angle of Projection. Set up the projector as specified by the manufacturer's written instructions. Draw an
are with a radius of 3 meters in the horizontal direction.
Using a small (less than 3 centimeters) photoelectric light
detector, measure the light intensity at 5-centimeter intervals on the are for 30 centimeters on either side of the
light source centerline of projection. Repeat the test in the
vertical direction. Then for both the horizontal and vertical directions, calculate the response of the photoelectric
detector as a function of the projection angle (26 centimeters of are with a radius of 3 meters equals 5 degrees).
report the relative angle of projection curves, and determine and report the angle of projection.
6.4 Optical Alignment Sight. In the laboratory set the
instrument up as specified by the manufacturer's written
instructions for a monitor path length of 8 meters. Align,
zero, and span the instrument. Insert an attenuator of 10
percent (nominal opacity) into the instrument path length.
Slowly misalign the projector unit by rotating it until a
positive or negative shift of 2 percent opacity is obtained
by the data recorder. Then, following the manufacturer's
written instructions, check the alignment. The alignment
procedure must indicate that the instrument is misaligned.
Repeat this test for lateral misaligmment of the projector.
Realign the instrument and follow the same procedure for
checking misalignment of the receiver or retroreflector
unit (lateral misalignment only).
6.5 Manufacturer's Certificate of Conformance (alternative to above). Obtain from the manufacturer a certificate of conformance stating that the first analyzer randomly sampled from each month's production was tested
according to Sections 6.1 through 6.4 and satisfactorily
met all requirements of Section 5 of this specification. If
any of the requirements were not met, the certificate must
state that the entire month's analyzer production was
resampled according to the military standard 105D sampling procedure (MIL-STD-105D) inspection level II:
was retested for each of the applicable requirements under
Section 5 of this specification: and was determined to be
acceptable under MIL-STD-105D procedures, acceptable
quality level 1.0. The certificate of conformance must include the results of each test performed for the analyzer(s)
sampled during the month the analyzer being installed
was produced.
7. Performance Specification Verification Procedure
Test each CEMS that conforms to the design specifications (Section 5.1) using the following procedures to determine conformance with the specifications of Table 1-
1. These tests are to be performed using the data recording system to be employed during monitoring. Prior approval from the Administrator is required if different data
recording systems are used during the performance test
and monitoring.
7.1 Preliminary Adjustments and Tests. Before installing the system on the stack, perform these steps or tests
at the affected facility or in the manufacturer's laboratory.
7.1.1 Equipment Preparation. Set up and calibrate the
CEMS for the monitor path length to be used in the installation as specified by the manufacturer's written instructions. For this specification, the mounting distance
between the transmitter and receiver/reflector unit at the
source must be measured prior to performing the calibrations (do not use distances from engineering drawings). If
the CEMS has automatic path length adjustment, follow
the manufacturer's instructions to adjust the signal output
from the analyzer in order to yield results based on the
emission outlet path length. Set the instrument and data
recording system ranges so that maximum instrument output is within the span range specified in the applicable
subpart.
Align the instrument so that maximum system response
is obtained during a zero (or upscale) check performed
across the simulated monitor path length. As part of this
alignment. include rotating the reflector unit (detector unit
for single pass instruments) on its axis until the point of
maximum instrument response is obtained.
Follow the manufacturer's instructions to zero and span
the instrument. Perform the zero alignment adjustment by
balancing the response of the CEMS so that the simulated
zero check coincides with the actual zero check performed across the simulated monitor path length. At this
time. measure and record the indicated upscale calibration
value. The calibration value reading must be within the
required opacity range (Section 3.3).
7.1.2 Calibration Attenuator Selection. Based on the
span value specified in the applicable subpart, select a
minimum of three calibration attenuators (low, mid, and
high range) using Table 1-2.
If the system is operating with automatic path length
compensation, calculate the attenuator values required to
obtain a system response equivalent to the applicable values shown in Table 1-2; use Equation 1-1 for the conversion. A series of filters with nominal optical density
(opacity) values of 0.1(20). 0.2(37), 0.3(50), 0.4(60),
0.5(68). 0.6(75), 0.7(80), 0.8(84), 0.9(88), and 1.0(90) are
commercially available. Within this limitation of filter
availability. select the calibration attenuators having the
values given in Table 1-2 or having values closest to
those calculated by Equation 1-1.
D₁=D₂ (L₁/L₂)
Eq. I-I
TABLE 1-2-REQUIRED CALIBRATION
ATTENUATOR VALUES (NOMINAL)
Calibrated attenuator optical density
Span value (percent
(equivatent opacity in parenthesis)-
opacity)
D2
Low-range
Mid-range
High-range
40
0.05 (11)
0.1 (20)
0.2 (37)
50
0.1 (20)
0.2 (37)
0.3 (50)
60
0.1 (20)
0.2 (37)
0.3 (50)
70
0.1 (20)
0.3 (50)
0.4 (60)
80
0.1 (20)
0.3 (50)
0.6 (75)
90
0.1 (20)
0.4 (60)
0.7 (80)
100
0.1 (20)
0.4 (60)
0.9 (87.5)
Where:
D1=Nominal optical density value of required mid, low,
or high range calibration attenuators.
D₂=Desired attenuator optical density output value from
Table 1-2 at the span required by the applicable subpart.
Pt. 60, App. B, Spec. 1
L₁=Monitor path length.
L₂=Emission outlet path length.
7.1.3 Attenuator Calibration. Select a laboratory calibration spectrophotometer meeting the specifications of