35 Ill. Adm. Code 370.845
High pH Stabilization
Section 370
Section 370.845 High pH
Stabilization
a) General
Alkaline material may be added to liquid primary or secondary
sludges for sludge stabilization in lieu of digestion facilities, to supplement
existing digestion facilities, or for interim sludge handling. Inasmuch as the
high pH stabilization process does not reduce organic matter but rather
increases the mass of dry sludge solids, so that additional volumes of sludge
will be generated in the absence of supplemental dewatering, the design shall
account for the increased sludge quantities for storage and handling,
transportation and disposal methods and associated costs. Alkaline material
may be added to dewatered sludges for stabilization pursuant to Section
370.520(b).
b) Operational Criteria
Sufficient alkaline material shall be added to liquid sludge
in order to produce a homogeneous mixture with a minimum pH of 12 after 2 hours
of vigorous mixing. Facilities for adding supplemental alkaline material shall
be provided to maintain the pH of the sludge during interim sludge storage
periods.
c) Odor Control and Ventilation
Odor control facilities shall be provided for sludge mixing
and treated sludge storage tanks that are located within ½ mile of residential
or commercial areas. Indoor sludge mixing, storage and processing facilities
shall have ventilation that meets the ventilation requirements contained in
Section 370.410(g)(1-4) and (6) and shall comply with the safety precautions
contained in Section 370.560. Adequate facilities shall be provided to
condition the exhaust air to meet the applicable substantive and permitting
requirements of 35 Ill. Adm. Code Subtitle B: Air Pollution.
d) Mixing Tanks and Equipment
1) Tanks
Mixing tanks may be designed to operate as either a batch or
continuous flow process. A minimum of two tanks of adequate size to provide a
minimum of 2 hours of contact time in each tank shall be provided. The
following factors shall also be taken into account in determining the number
and size of tanks:
A) Peak sludge flow rates;
B) Storage between batches;
C) Dewatering or thickening performed in tanks;
D) Repeating sludge treatment due to pH decay of stored sludge;
E) Sludge thickening prior to sludge treatment;
F) Type of mixing device used and associated maintenance and
repair requirements.
2) Equipment
Mixing equipment shall be designed to provide vigorous
agitation within the mixing tank, to maintain solids in suspension and to
provide for a homogenous mixture of the sludge solids and alkaline material.
Mixing may be accomplished by either diffused aeration or mechanical mixing.
For diffused aeration, an air supply of 30 cfm per 1000 cubic feet of mixing
tank volume with the largest blower out of service shall be provided.
Nonclogging diffusers designed to permit continuity of service should be used.
Mechanical mixers shall be designed to assure continuity of service during
freezing weather conditions and shall be equipped with impellers designed to
minimize fouling from debris in the sludge.
e) Chemical Feed and Storage Equipment
1) General
Equipment used for handling or storing alkaline shall be
designed to provide operator protection from eye and tissue damage. Refer to
Section 370.560 for proper safety precautions. Material storage, slaking and
feed equipment shall be sealed as airtight as practicable to prevent contact of
alkaline material with atmospheric carbon dioxide and water vapor and to
prevent the escape of dust material. All equipment and associated transfer
lines and piping shall be accessible for cleaning.
2) Feed and Slaking Equipment
The design of the feeding equipment shall be determined by
the treatment plant size, type of alkaline material used, slaking required and
operator requirements. Automated or batch equipment may be used. Automated
feeders may be volumetric or gravimetric, based on accuracy, reliability and
maintenance requirements. Manually operated batch slaking of quicklime (CaO)
should be avoided unless protective clothing and equipment are provided. At
small plants, for safety reasons the use of hydrated lime (Ca(OH)[2]) over
quicklime is recommended. Feed and slaking equipment shall be sized to handle
a minimum of 150% of the peak sludge flow rate, including sludge that may need
to be retreated due to pH decay. Duplicate units shall be provided.
3) Chemical Storage Facilities
Alkaline materials may be received in either bag or bulk
form. Materials delivered in bags must be stored indoors and elevated above
floor level. Bags should be multi-walled and moisture-proof. Dry bulk storage
containers must be as airtight as practicable and shall contain a mechanical
agitation mechanism. Storage facilities shall be sized to provide a minimum
30-day supply of alkaline materials. Adequate provisions shall be made to meet
the applicable substantive and permitting requirements of 35 Ill. Adm. Code
Subtitle B: Air Pollution.
f) Sludge Storage
Refer to Section 370.870 for general design considerations
for sludge storage facilities. The design shall incorporate the following
considerations for the storage of high pH stabilized sludge:
1) Liquid Sludge
Liquid high pH stabilized sludge shall be stored in a tank or
vessel equipped with rapid sludge withdrawl mechanisms for sludge disposal or
retreatment and may not be stored in a lagoon. Provision shall be made for
adding alkaline material in the storage tank. Mixing equipment meeting the
requirements of subsection (d)(2) above shall be provided in all storage tanks.
2) Dewatered Sludge
On-site storage of dewatered high pH stabilized sludge shall
be limited to 30 days. Provisions shall be made for rapid retreatment or
disposal of dewatered sludge stored on site in case of sludge pH decay.
3) Off-Site Storage
There shall be no off-site storage of high pH stabilized
sludge unless the Agency has issued a permit for off-site storage.
g) Disposal
Methods and options for immediate sludge disposal should be
used in order to reduce the on-site sludge inventory and the amount of sludge
that must be retreated to reduce odors when sludge pH decay occurs. Where land
application is used, the sludge must be incorporated into the soil within 24
hours after application.